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- Chemical and Mineralogical Characterization ofWaste from Abandoned Copper and Manganese Mines in the Iberian Pyrite Belt, Portugal: A First Step Towards the Waste-to-Value Recycling ProcessPublication . de Oliveira, Daniel Pipa Soares; Silva, Teresa; Morais, Igor; Fernandes, JoãoABSTRACT: This study examines the chemical and mineralogical composition of waste materials from abandoned copper and manganese mines in the Iberian Pyrite Belt, Portugal, as a first step toward their potential recycling for critical and strategic raw materials (CRM and SRM). Using portable X-ray fluorescence (pXRF) and other analytical techniques, this research highlights the presence of valuable elements, including copper, manganese, and rare earth elements, in concentrations significantly above their crustal abundance. The findings underscore the dual potential of these wastes: as sources of secondary raw materials and for mitigating environmental hazards such as acid mine drainage (AMD). Recovered materials include chalcopyrite, pyrolusite, and rhodochrosite, with critical elements like cobalt, lithium, and tungsten identified. pXRF proved to be a reliable, cost effective tool for rapid field and laboratory analyses, demonstrating high precision and good correlation with standard laboratory methods. The study emphasizes the importance of characterizing historical mining waste to support a circular economy, reduce reliance on foreign material imports, and address environmental challenges. This approach aligns with the European Union’s Critical Raw Materials Act, promoting sustainable resource use and the recovery of strategic resources from historical mining sites.
- Decision criteria for the exploration of ornamental-stone deposits: Application to the marbles of the Portuguese Estremoz AnticlinePublication . Falé, Patrícia; Carvalho, Jorge; Henriques, Paulo; Luís, GabrielABSTRACT: Ornamental stones are almost ready-made raw materials with a high economic value for the building-construction industry. The discovery of new near-surface deposits, the very low exploitation efficiency, the huge amounts of wastes produced, and the land-use accessibility conditions are the main challenges that the extractive industry for this mineral resource is facing nowadays. Research on advanced geological exploration tools and methodologies is needed to reply to those challenges. During the process of geological ornamental-stone deposits exploration, the unique and decisive criteria that should be considered are its dimensions, homogeneity, and fracturing state. Lithostructural geological mapping and in situ fracturing surveys are the basic indispensable tools for their field assessment. By applying these criteria and tools to a marble-rich area in the Portuguese Estremoz Anticline and a step-by-step numerical evaluation of the qualitative geological parameters, the delimitation of the best target areas for exploitation or environmental rehabilitation has been effectively mapped.
- New Contributions to Mineralogical and Geochemical Knowledge of Old Preguiça Mine, Beja, PortugalPublication . Silva, Teresa; Morais, Igor; Mesquita Soares, Sofia; Rodrigues, Ivo; de Oliveira, Daniel Pipa Soares; Mirao, JoseABSTRACT: Abandoned mining areas provide valuable opportunities to investigate ore-forming processes, supergene mineral transformations, and the geochemical behaviour of metals. In this sense, the old Preguiça mine (Beja, Portugal), exploited for Fe–Zn–Pb, was studied providing new mineralogical and geochemical data aimed at improving the understanding of the secondary mineral assemblages of this deposit. A total of 70 samples collected from three accessible underground levels (first, second and third) and mine waste, complemented by 16 samples from a deeper level (fourth) previously collected, were analysed using X-ray diffraction (XRD), scanning electron microscopy (SEM), and a portable X-ray fluorescence (pXRF) equipment. Mineralogical phases are dominated by a wide range of secondary oxides, carbonates, arsenates, vanadates, silicates, phosphates and sulphates, but remnants of primary sulphides were also found. The following minerals can be emphasised: goethite, hematite, calcite, dolomite, descloizite, willemite, mimetite, cerussite, smithsonite and fraipontite. The presence of massicot in the Preguiça mine, is described for the first time. Bulk geochemical analyses show high concentrations of Fe, Ca, Zn and Pb, consistent with the observed mineralogy. The presence of vanadium- and arsenic-bearing minerals highlights the occurrence of critical raw materials, supporting the importance of reassessing other abandoned mining areas in the context of sustainable resource management and strategic raw-material planning.